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Visualizing time-dependent microstructural and chemical evolution during molten salt corrosion of Ni-20Cr model alloy using c...

Publication Type
Journal
Journal Name
Corrosion Science
Publication Date
Page Number
109962
Volume
195

In situ monitoring of corrosion processes is important to fundamentally understand the kinetics and evolution of materials in harsh environments. A quasi in situ transmission electron microscopy technique was utilized to study microstructural and chemical evolution of a Ni-20Cr disc sample exposed to molten KCl-MgCl2 salt for 60 s in consecutive 20 s iterations. In situ synchrotron X-ray nano-tomography was performed to characterize the morphological evolution of a Ni-20Cr microwire exposed to molten KCl-MgCl2. Both techniques captured key corrosion events and revealed mechanisms at different time and length scales, potentially bringing greater insights and deeper understanding beyond conventional analysis.