Skip to main content
SHARE
Publication

Deoxygenation of Unhindered Alcohols via Reduction of Derived Phosphate Esters...

by Sarwat Chowdhury, Robert F Standaert
Publication Type
Journal
Journal Name
Journal of Organic Chemistry
Publication Date
Volume
81
Issue
20

Primary alcohols can be deoxygenated cleanly and in high yield by reduction of derived diphenyl phosphate esters with lithium triethylborohydride in tetrahydrofuran at room temperature. Selective deoxygenation of a primary alcohol in the presence of a secondary alcohol was demonstrated. The two-step process can be performed in one pot, making it simple and convenient.