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Deuterium incorporation in biomass cell wall components by NMR analysis...

by Marcus B Foston, Joseph Mcgaughey, Hugh M O'neill, Barbara R Evans, Arthur J Ragauskas
Publication Type
Journal
Journal Name
Analyst, The
Publication Date
Page Numbers
1090 to 1093
Volume
137
Issue
5

A commercially available deuterated kale sample was analyzed for deuterium incorporation by ionic liquid solution 2H and 1H nuclear magnetic resonance (NMR). This protocol was found to effectively measure the percent deuterium incorporation at 33%, comparable to the 31% value determined by combustion. The solution NMR technique also suggested by a qualitative analysis that deuterium is preferentially incorporated into the carbohydrate components of the kale sample.