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Extraction of flow properties of single crystal silicon carbide by nanoindentation and finite element simulation...

by Sang Hoon Shim, Jae-il Jang, George M Pharr
Publication Type
Journal
Journal Name
Acta Materialia
Publication Date
Page Numbers
3824 to 3832
Volume
56
Issue
15

A method is presented for estimating the plastic flow behavior of single crystal silicon carbide by nanoindentation experiments using a series of triangular pyramidal indenters with different centerline-to-face angles (35.3?to 75?in this work) in combination with 2-dimensional axisymmetric finite element (FE) simulations. The method is based on Tabor's concepts of characteristic strain, e_char, and constraint factor, C_q, which allow indentation hardness values obtained with indenters of different angles to be related to the flow properties of the indented material. The procedure utilizes FE simulations applied in an iterative manner in order to establish the yield strength and work hardening exponent from the experimentally measured dependence of the hardness on indenter angle. The methodology is applied to a hard, brittle ceramic material, 6H SiC, whose flow behavior cannot be determined by conventional tension or compression testing. It is shown that the friction between the indenter and the material plays a significant role, especially for very sharp indenters.