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A review of advantages of high-efficiency X-ray spectrum imaging for analysis of nanostructured ferritic alloys...

by Chad M Parish, Michael K Miller
Publication Type
Journal
Journal Name
Journal of Nuclear Materials
Publication Date
Page Numbers
433 to 442
Volume
462

Nanostructured ferritic alloys (NFAs) exhibit complex microstructures consisting of 100-500 nm ferrite grains, grain boundary solute enrichment, and multiple populations of precipitates and nanoclusters (NCs). Understanding these materials' excellent creep and radiation-tolerance properties requires a combination of multiple atomic-scale experimental techniques. Recent advances in scanning transmission electron microscopy (STEM) hardware and data analysis methods have the potential to revolutionize nanometer to micrometer scale materials analysis. The application of these methods is applied to NFAs as a test case and is compared to both conventional STEM methods as well as complementary methods such as scanning electron microscopy and atom probe tomography. In this paper, we review past results and present new results illustrating the effectiveness of latest-generation STEM instrumentation and data analysis.